Table 4 1H (700 MHz) and 13CNMR (175 MHz) spectroscopic data for Griseococcin (1): in DMSO
From: Griseococcin (1) from Bovistella radicata (Mont.) Pat and antifungal activity
Position | δ H (mult, J inHz) | δC |
|---|---|---|
1 | 7.81 | 166 |
2 | 128.56 | |
3 | 175.11 | |
4 | 138.60 | |
5 | 7.93 | 135.7 |
6 | 7.72 | 137.21 |
7 | 136.28 | |
8 | 7.80 | 135.45 |
9 | 138.56 | |
10 | 175.07 | |
11 | 128.57 | |
12 | 7.66 | 166.07 |
13 | 1.07 | 30.18 |
14 | 3.62 | 166.01 |
15 | 3.49 | 166.02 |
16 | 3.55 | 166.03 |
17 | 3.51 | 166.01 |
18 | 1.25 | 23.15 |
19 | 1.94 | 23.16 |
20 | 2.09 | 184.15 |
1′ | 1.94 | 28.4 |
2′ | 215.7 | |
3′ | 2.14 | 23.4 |
4′ | 4.47 | 73.6 |
4′-OH | 8.37 | |
5′ | 2.12 | 29.05 |
6′ | 215.7 | |
7′ | 1.08 | 25.52 |
8′ | 1.94 | 26.81 |
9′ | 3.62 | 71.25 |
9′-OH | 7.81 | |
10′ | 1.29 | 23.45 |
11′ | 3.49 | 71.15 |
11′-OH | 7.80 | |
12′ | 1.73 | 23.47 |
13′ | 3.51 | 71.18 |
13′-OH | 7.93 | |
14′ | 1.85 | 20.27 CH3 |
15′ | 2.11 | 20.27 CH3 |
16′ | 1.06 | 20.27 CH3 |
17′ | 1.07 | 20.27 CH3 |