Table 4 1H and 13C NMR data for the major compound in the F3 fraction
Position | δC, mult | δH, mult (J in Hz) |
|---|---|---|
1 | 175.5, s | – |
2 | 35.9, t | 2.22, t (8.0) |
3 | 25.5, t | 1.63, m |
4 | 29.2, t | 1.26, br s |
5 | 29.3, t | |
6, 7, 8 | 29.5, t | |
9 | 29.5, t | |
10 | 29.6, t | |
11 | 29.6, t | |
16 | 29.7, t | |
17,18 | 29.8, t | |
19 | 29.5, t | |
20 | 31.9, t | |
21 | 22,7, t | |
12,15 | 27.2, t | 2.01, dd (12.1, 6.4) |
13 | 129.9, d | 5.36, t (4.7) |
14 | 129.9, d | |
22 | 14.1, q | 0.88, t (6.7) |