DsLOV “dark” | DsLOV “photoexcited” | |
---|---|---|
Wavelength (Å) | 0.93340 (Beamline: ESRF, ID14-1) | 0.95372 (Beamline: ESRF, ID23-1) |
Detector type | ADSC Quantum Q210 | ADSC Quantum Q315r |
Resolution range (Å) | 45.4 - 1.5 (1.53 - 1.5)a | 26.1 - 2.0 (2.07 - 2.0)a |
Space group | C 1 2 1 | C 1 2 1 |
Unit cell | a = 89.98 (Å) | a = 90.78 (Å) |
b = 30.60 (Å) | b = 30.94 (Å) | |
c = 49.33 (Å) | c = 49.54(Å) | |
β = 113.03° | β = 113.09° | |
Total reflections | 65088 | 30165 |
Unique reflections | 19912 | 8206 |
Multiplicity | 3.3 (2.5) | 3.7 (4.0) |
Completeness (%) | 98.98 (91.59) | 93.48 (98.15) |
Mean I/σ (I) | 19.7 (4.3) | 16.3 (10.4) |
Wilson B-factor (Å2) | 14.08 | 10.62 |
R-sym | 0.037 (0.203) | 0.061 (0.085) |
R-work | 0.1298 (0.1115) | 0.1633 (0.1595) |
R-free | 0.1789 (0.2031) | 0.1824 (0.1586) |
Coordinate error (maximum-likelihood based) (Å) | 0.13 | 0.16 |
Number of atoms | 1125 | 1015 |
Macromolecules | 981 | 904 |
Ligands | 32 | 27 |
Water molecules | 112 | 84 |
Protein residues | 120 | 115 |
RMS (bonds) (Å) | 0.014 | 0.004 |
RMS (angles) (°) | 1.56 | 0.77 |
Ramachandran favored (%) | 99 | 99 |
Ramachandran outliers (%) | 0 | 0 |
Clash score | 2.99 | 4.92 |
Average B-factor (Å2) | 19.9 | 14.7 |
PDB entry | 4KUK | 4KUO |